Geetanjali Lohiya; Anshu Tamta; Bhuwan Chandra; Narain Datt Kandpal; Rajendra Joshi
Abstract
Nanoparticles of manganese oxide have been synthesized by a green chemistry approach using manganese chloride (MnCl2.2H2O), potassium permanganate (KMnO4), and methanolic extract of Sapindus mukorossi (reetha). In this study, we report here a simple ecofriendly green route to synthesize MnO2 nanoparticles. ...
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Nanoparticles of manganese oxide have been synthesized by a green chemistry approach using manganese chloride (MnCl2.2H2O), potassium permanganate (KMnO4), and methanolic extract of Sapindus mukorossi (reetha). In this study, we report here a simple ecofriendly green route to synthesize MnO2 nanoparticles. Manganese oxide nanoparticles were characterized by Fourier Transform Infra-Red (FTIR), UV-Vis spectral analysis, High-Resolution Transmission Electron Microscope (HRTEM), and Scanning Electron Microscope (SEM). The surface morphology showed that the MnO2 nanoparticles were uniformly dispersed. The average particle size was found 16 nm obtained by X-ray Diffraction (XRD), analysis. To find particle size DLS analysis has been done. The thermal stability of the nanoparticles with the temperature increase has been determined by Thermo-gravimetric Analysis (TGA) measurement. The synthesized manganese oxide nanoparticles were screened for antibacterial activities on gram-positive bacteria Staphylococcus aureus, Bacillus subtilis, and gram negative bacteria Pseudomonas aeruginosa, Escherichia coli. The results of the antibacterial study suggest that the manganese oxide nanoparticles can be useful for effective growth inhibitors in microorganisms with applications to medical devices and antimicrobial-controlled systems. The order of the reactivity towards zone of inhibition of microorganisms observed in the order of Escherichia coli (9mm) > Pseudomonas aeruginosa (8.3mm) > Bacillus subtilis (7.3mm) > Staphylococcus aureus (5.3mm).
P. Koteswara Rao; B Vikram Babu; A. Rama Krishna; M. Sushma Reddi; B. Sathish Mohan; K. Anjani Devi; U. Susmitha; T. Raghava Rao
Abstract
The present study explores the green approach for the preparation of silver nanoparticles (AgNPs) through the reduction of silver nitrate by the cell-free stem and leaf aqueous extracts of Litsea glutinosa (L.glutinosa) and its potential antibacterial activity. The analytical instruments include scanning ...
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The present study explores the green approach for the preparation of silver nanoparticles (AgNPs) through the reduction of silver nitrate by the cell-free stem and leaf aqueous extracts of Litsea glutinosa (L.glutinosa) and its potential antibacterial activity. The analytical instruments include scanning electron microscopy, Fourier transforms infrared spectroscopy, UV-visible spectroscopy, and X-ray diffraction spectroscopy confirmed the synthesis of smaller, uniformly spherical AgNPs (10-40 nm). The average crystalline size of prepared AgNPs produced by L. glutinosa leaf extract was found to be 19 mm. From UV-visible spectral analysis, the maximum absorbance peak appeared at 444 nm for leaf extract AgNPs different from stem extract AgNPs (422 nm), which are found to be specific for AgNPs. The L.glutinosa stem extract-assisted AgNPs have shown significant antibacterial activity against Bacillus subtilis (Gram-positive) and Escherichia coli (Gram-negative) in comparison to Gentamycin. Hence, the AgNPs obtained by green synthesis can be therapeutically explored against bacterial infections.
Ananda A; Ramakrishnappa T; Ravishankar T N; Archana S; Shilpa B M; Reddy yadav L S; Jayanna B K
Abstract
In this work, the tetragonal Zirconium oxide (ZrO2) nanoparticles (NPs) were successfully synthesized by solution combustion method using Zirconium (IV) oxynitrate hydrate as the metal precursor and an oxidizer, Basella alba raw extract at 6000C. In this study, natural fuel is used to avoid harmful chemical ...
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In this work, the tetragonal Zirconium oxide (ZrO2) nanoparticles (NPs) were successfully synthesized by solution combustion method using Zirconium (IV) oxynitrate hydrate as the metal precursor and an oxidizer, Basella alba raw extract at 6000C. In this study, natural fuel is used to avoid harmful chemical fuels that may pollute the environment during combustion. The impact of the fuel-to-oxidant molar ratio on the surface morphological features of nanocrystalline zirconia particles has been documented. We investigated the Physico-chemical properties of the ZrO2 NPs via thorough characterizations like XRD, EDS, SEM, TEM, FTIR, UV-Vis, and BET. ZrO2 NPs exhibit perfect photocatalytic degradation activity towards Evans blue, a toxic dye. The influence of contact time, initial dye concentration, and pH were among the independent variables used in the study. The Response Surface Model (RSM) was used to optimize and describe the interdependencies of the different variables. The method was evaluated using the Box-Behnken design (BBD). A second-order polynomial model was used to properly understand the experimental results, and the effectiveness of the chosen model was verified by the strong agreement in determination coefficient values. ZrO2 NPs also exhibit good antibacterial activity on Gram-negative Klebsiella pneumoniae and Gram-positive bacteria, Bacillus subtilis.
Sathiya Sheela D; P Viswanathan; K Kalimuthu; A Vanitha
Abstract
The development of biologically enthused green synthesis of silver nanoparticles (SNPs) has concerned significant global awareness about medical science and disease treatment. This paper discusses the green synthesis of SNPs using organic green sources; here we report a facile bottom-up ‘green’ ...
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The development of biologically enthused green synthesis of silver nanoparticles (SNPs) has concerned significant global awareness about medical science and disease treatment. This paper discusses the green synthesis of SNPs using organic green sources; here we report a facile bottom-up ‘green’ route for the synthesis of SNPs using aqueous leaves extract of Pogostemon speciosus (Benth.) and evaluate its in-vitro anti-inflammatory, antibacterial and photocatalytic activities. The nanoparticles were investigated for the preparation of denaturation particles with PSLASNPs and the evaluation of anti-inflammatory activity with Protein denaturation and HRBC stabilization assays. Later, these PSLASNPs were studied for their potential role in antibacterial activity by well diffusion method, and Photocatalytic activity on degradation of dyes was demonstrated by using dyes Crystal violet, Coomassie blue, and Congo red. At 1000 µg/ml, the PSLASNPs have the greatest prevention of protein denaturation (71.92±1.37%), whilst the stabilization of the HRBC membrane exhibited significant anti-inflammatory action (64.39±1.61 %). The PSLASNPs showed the best antibacterial activity at the concentration of 10 µg/ml against Bacillus subtilis (8.2 mm), followed by Pseudomonas stuberia (6.2 mm) and Escherichia coli (6.4 mm), Staphylococcus aureus (5.3 mm), Staphylococcus gallinarium (4.5 mm) respectively at the same concentrations. Crystal violet, Coomassie blue, and Congo red were used for Photocatalytic activity on the breakdown of dyes. After 35 minutes, the degradation process was determined to be complete by the transformation of the reaction mixture's color to colorless. As a result, the PSLASNPs have anti-inflammatory, antibacterial, and photocatalytic activities.